乙酸-3-甲基-3-丁烯-1-醇酯合成路线 (共 36 条)
参考文献
Ostromysslenski
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1915 , vol. 47, p. 1982
Chem. Zentralbl., 1916 , vol. 87, # II p. 307
反应条件
N-ethyl-N,N-diisopropylamine T=70°C; 20 h; with other hintered amines too; Product distribution;
参考文献
Badet, B.; Julia, M.; Marazano, C.
Tetrahedron Letters, 1985 , vol. 26, # 16 p. 2007 - 2010
反应条件
pyridine; sulfuryl dichloride; lithium perchlorate in dichloromethane T=-60°C; 0.333333 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Veselovskii, V. V.; Skorobogatov, S. P.; Novikova, M. A.; Moiseenkov, A. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 3.1 p. 513 - 516
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 3 p. 591 - 594
反应条件
trifluoroacetic acid in nitromethane T=0°C; 2 h; Further byproducts given;
参考文献
Julia, M.; Schmitz, C.
Tetrahedron, 1986 , vol. 42, # 9 p. 2485 - 2490
反应条件
trifluoroacetic acid in nitromethane T=0°C; 1 h; Product distribution;
参考文献
Julia, M.; Schmitz, C.
Tetrahedron, 1986 , vol. 42, # 9 p. 2485 - 2490
反应条件
trifluoroacetic acid in nitromethane T=0°C; 1 h; Product distribution;
参考文献
Julia, M.; Schmitz, C.
Tetrahedron, 1986 , vol. 42, # 9 p. 2485 - 2490
反应条件
trifluoroacetic acid in nitromethane T=0°C; 2 h; Product distribution;
参考文献
Julia, M.; Schmitz, C.
Tetrahedron, 1986 , vol. 42, # 9 p. 2485 - 2490
参考文献
Journal of the American Chemical Society, , vol. 77, p. 78
Justus Liebigs Annalen der Chemie, , vol. 630, p. 58,70
反应条件
1: 81 percent / HBF4*Et2O / CH2Cl2 / -30 °C 2: 10N NaOH / CH2Cl2; methanol / 24 h / Ambient temperature View Scheme
参考文献
Badet, B.; Julia, M.; Mallet, J. M.; Schmitz, C.
Tetrahedron Letters, 1983 , vol. 24, # 30 p. 4331 - 4334
反应条件
methanesulfonic acid in nitromethane T=0°C; 1.5 h;
参考文献
Julia, M.; Schmitz, C.
Tetrahedron, 1986 , vol. 42, # 9 p. 2485 - 2490