2-(乙酰基氨基)-5-氯苯甲酸合成路线 （共 10 条）
参考文献
Magidson; Trawin
Zhurnal Obshchei Khimii, 1937 , vol. 7, p. 842,844
Chem. Zentralbl., 1939 , vol. 110, # I p. 1366
反应条件
1: 92 percent / acetic anhydride / 3 h / Heating 2: 90 percent / aq. NH3 / ethanol / 48 h / 20 °C View Scheme
参考文献
Santagati, Natale Alfredo; Bousquet, Ennio; Spadaro, Angelo; Ronsisvalle, Giuseppe
Farmaco, 1999 , vol. 54, # 11-12 p. 780 - 784
反应条件
1: 2.0 g / cc. nitric acid / H2SO4 / 1 h / 0 °C 2: 1.40 g / cc. hydrochloric acid / H2O / 1 h / Heating 3: 1.8 g / stannous chloride dihydrate / HCl / 100 °C 4: 1.6 g / H2, KOH / Raney nickel / ethanol 5: 2.) sodium carbonate, deactivated Raney Ni / 1.) acetic acid, water (1:1), 15 min, warming; 2.) water, 70 deg C, 3 h View Scheme
参考文献
Deady, Leslie W.; Kaye, Anthony J.
Australian Journal of Chemistry, 1997 , vol. 50, # 5 p. 473 - 478
反应条件
acetic anhydride
Cyclization; 3 h; Heating;
参考文献
Santagati, Natale Alfredo; Bousquet, Ennio; Spadaro, Angelo; Ronsisvalle, Giuseppe
Farmaco, 1999 , vol. 54, # 11-12 p. 780 - 784
反应条件
1: 2.0 g / cc. nitric acid / H2SO4 / 1 h / 0 °C
2: 1.40 g / cc. hydrochloric acid / H2O / 1 h / Heating
View Scheme
参考文献
Deady, Leslie W.; Kaye, Anthony J.
Australian Journal of Chemistry, 1997 , vol. 50, # 5 p. 473 - 478
参考文献
Tomisek; Christensen
Journal of the American Chemical Society, 1948 , vol. 70, p. 2423
参考文献
Tomisek; Christensen
Journal of the American Chemical Society, 1948 , vol. 70, p. 2423
反应条件
potassium permanganate; magnesium sulfate
参考文献
Magidson; Trawin
Zhurnal Obshchei Khimii, 1937 , vol. 7, p. 842,844
Chem. Zentralbl., 1939 , vol. 110, # I p. 1366
反应条件
in acetic acid
0.5 h; Heating;
参考文献
Deady, Leslie W.; Kaye, Anthony J.
Australian Journal of Chemistry, 1997 , vol. 50, # 5 p. 473 - 478
反应条件
1: aqueous acetic acid; sodium chlorate; aqueous hydrochloric acid
2: aqueous potassium permanganate; magnesium sulfate
View Scheme
参考文献
Magidson; Trawin
Zhurnal Obshchei Khimii, 1937 , vol. 7, p. 842,844
Chem. Zentralbl., 1939 , vol. 110, # I p. 1366
