L-半胱氨酸盐酸盐无水物合成路线 (共 109 条)
反应条件
hydrogenchloride; water 24 h; Inert atmosphereReflux;
参考文献
Mercey, Guillaume; Bregeon, Delphine; Gaumont, Annie-Claude; Levillain, Jocelyne; Gulea, Mihaela
Tetrahedron Letters, 2008 , vol. 49, # 46 p. 6553 - 6555
反应条件
hydrogenchloride 168 h;
参考文献
Threadgill, Michael D.; Gledhill, Adrian P.
Journal of Organic Chemistry, 1989 , vol. 54, # 12 p. 2940 - 2949
反应条件
hydrogenchloride; water T=110°C; 24 h;
参考文献
Tan, Karen Co; Wakimoto, Toshiyuki; Takada, Kentaro; Ohtsuki, Takashi; Uchiyama, Nahoko; Goda, Yukihiro; Abe, Ikuro
Journal of Natural Products, 2013 , vol. 76, # 7 p. 1388 - 1391
反应条件
mercury(II) diacetate in water; acetic acid 0.25 h; other reagent (zinc dust, 80percent acetic acid, 15 min); Product distribution;
参考文献
Coyle, Susan; Hallett, Allan; Munns, Michael S.; Young, Geoffrey T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 522 - 528
反应条件
(i) CuCl, aq. H2SO4, (ii) benzenediazonium salt; Multistep reaction;
参考文献
Wolfe,S. et al.
Canadian Journal of Chemistry, 1979 , vol. 57, # 18 p. 2412 - 2425
反应条件
sodium hydroxide in ethanol; water 48 h; Ambient temperature;
参考文献
Zheng, Guo-qiang; Kenney, Patrick M.; Lam, Luke K. T.
Journal of Medicinal Chemistry, 1992 , vol. 35, # 1 p. 185 - 188
参考文献
Friedman,M. et al.
Journal of the American Chemical Society, 1965 , vol. 87, p. 3672 - 3682
反应条件
1: L-cysteine monohydrochloride powder With hydrogenchloride; sodium nitrite T=5°C; 1 h; 2: methanesulfinic acid sodium salt T=5°C; 14 h;
参考文献
Leonov, Andrei; Voigt, Brigitte; Rodriguez-Castaneda, Fernando; Sakhaii, Peyman; Griesinger, Christian
Chemistry - A European Journal, 2005 , vol. 11, # 11 p. 3342 - 3348
反应条件
barium dihydroxide in ethanol
参考文献
Marrone; Siemann; Beecroft; Viswanatha
Bioorganic Chemistry, 1996 , vol. 24, # 4 p. 401 - 416
反应条件
1: 2,4,5,6-tetraaminopyrimidine sulphate With BaCl2 in water T=90°C; 0.25 h; 2: L-cysteine monohydrochloride powder With ammonium hydroxide; oxygen; ammonium chloride in water T=5°C; 0.25 h; 3: With 1,3-dihydroxy-2-propanone-dimer; oxygen in water T=5 - 20°C; 48 h; Further stages.;
参考文献
Valiaeva; Bartley; Konno; Coward
Journal of Organic Chemistry, 2001 , vol. 66, # 15 p. 5146 - 5154