2,3’,4,4’,6-五羟基二苯甲酮合成路线 （共 13 条）
反应条件
aluminium trichloride; toluene T=120°C;
参考文献
Russell; Butler
Journal of the American Chemical Society, 1949 , vol. 71, p. 3663
反应条件
hydrogenchloride; diethyl ether; zinc(II) chloride T=50 - 60°C; man loest das Reaktionsprodukt in Wasser,neutralisiert die waessr.Loesung mit Ammoniak und kocht sie 2 Stdn.;
参考文献
Fujita, Masao; Inoue, Takao
Chemical & Pharmaceutical Bulletin, 1980 , vol. 28, # 8 p. 2482 - 2486
反应条件
1: 60 percent KOH / 2.5 h / 100 °C / labelled comp. 2: fused ZnCl2, dry HCl / diethyl ether / 3 h / 60 °C / labelled comp. View Scheme
参考文献
Fujita, Masao; Inoue, Takao
Chemical & Pharmaceutical Bulletin, 1980 , vol. 28, # 8 p. 2482 - 2486
反应条件
1: KOH-NaOH / 1 h / 290 - 300 °C / labelled comp. 2: fused ZnCl2, dry HCl / diethyl ether / 3 h / 60 °C / labelled comp. View Scheme
参考文献
Fujita, Masao; Inoue, Takao
Chemical & Pharmaceutical Bulletin, 1980 , vol. 28, # 8 p. 2482 - 2486
反应条件
1: HI (d=1.7) / 2.5 h / Heating; labelled comp. 2: KOH-NaOH / 1 h / 290 - 300 °C / labelled comp. 3: fused ZnCl2, dry HCl / diethyl ether / 3 h / 60 °C / labelled comp. View Scheme
参考文献
Fujita, Masao; Inoue, Takao
Chemical & Pharmaceutical Bulletin, 1980 , vol. 28, # 8 p. 2482 - 2486
反应条件
Erhitzen oberhalb des Schmelzpunkts;
参考文献
Smith
Journal and Proceedings of the Royal Society of New South Wales, 1896 , vol. 30, p. 135,136
参考文献
Wagner
Journal fuer Praktische Chemie (Leipzig), 1850 , vol. <1> 51, p. 95
Journal fuer Praktische Chemie (Leipzig), 1851 , vol. <1> 52, p. 449
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Wagner
Jahresbericht ueber die Fortschritte der Chemie und Verwandter Theile Anderer Wissenschaften, 1850 , p. 531
Jahresbericht ueber die Fortschritte der Chemie und Verwandter Theile Anderer Wissenschaften, 1851 , p. 419
参考文献
Benedikt
Justus Liebigs Annalen der Chemie, 1877 , vol. 185, p. 118
参考文献
Hlasiwetz; Pfaundler
Justus Liebigs Annalen der Chemie, 1863 , vol. 127, p. 357
反应条件
culture biomass of Rhodotorula buffonii in aq. phosphate buffer; N,N-dimethyl-formamide 24 h; Microbiological reactionHeating; Time;
参考文献
Fromentin, Yann; Grellier, Philippe; Buisson, Didier; Lallemand, Marie-Christine; Wansi, Jean Duplex
Organic Letters, 2012 , vol. 14, # 19 p. 5054 - 5057,4
