in acetonitrile
under N2, addn. of solid Na(SCH3) to a soln. of NiCl2 in CH3CN, after 20 h removal of pptd. Ni, addn. of excess of solid (N(CH3)4)Cl to the filtrate, a few days at room temp.; filtration, washed with diethyl ether, dried in vac.; elem. anal.;
参考文献
Henkel, Gerald; Kriege, Michael; Matsumoto, Keiji
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1988 , p. 657 - 660
