N'-[1,6-二氢-4-甲基-5-硝基-6-氧代-1-[(苯基甲氧基)甲基]-2-嘧啶基]-N,N-二甲基甲脒合成路线 （共 3 条）
反应条件
1: 91 percent / dimethylformamide / 40 h / 20 °C 2: 95 percent / sodium hydrogen sulfite / tetrahydrofuran; H2O / 12 h / 20 °C 3: 95 percent / ammonia / ethanol / 4 h / 165 - 170 °C 4: 90 percent / hydrogen / palladium(II) hydroxide on carbon / methanol / 5 h / 2585.74 Torr View Scheme
参考文献
Liu, Mao-Chin; Luo, Mei-Zhen; Mozdziesz, Diane E.; Sartorelli, Alan C.
Synthetic Communications, 2002 , vol. 32, # 24 p. 3797 - 3802
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in N,N-dimethyl-formamide
T=20°C; 2 h;
参考文献
Liu, Mao-Chin; Luo, Mei-Zhen; Mozdziesz, Diane E.; Sartorelli, Alan C.
Synthetic Communications, 2002 , vol. 32, # 24 p. 3797 - 3802
反应条件
1: 91 percent / dimethylformamide / 40 h / 20 °C
2: 95 percent / sodium hydrogen sulfite / tetrahydrofuran; H2O / 12 h / 20 °C
3: 95 percent / ammonia / ethanol / 4 h / 165 - 170 °C
View Scheme
参考文献
Liu, Mao-Chin; Luo, Mei-Zhen; Mozdziesz, Diane E.; Sartorelli, Alan C.
Synthetic Communications, 2002 , vol. 32, # 24 p. 3797 - 3802
