1,2-二碘-4,5-二甲基苯合成路线 (共 6 条)
反应条件
1: With pyridine; potassium permanganate in water 48 h; Reflux; 2: With potassium hydroxide in water Heating; 3: With hydrogenchloride in water pH=1 - 2;
参考文献
Dudic, Miroslav; Cisarova, Ivana; Michl, Josef
Journal of Organic Chemistry, 2012 , vol. 77, # 1 p. 68 - 74
反应条件
iodine; acetic acid; periodic acid; sulfuric acid
T=70°C;
参考文献
Kovalenko, Serguei V.; Peabody, Scott; Manoharan, Mariappan; Clark, Ronald J.; Alabugin, Igor V.
Organic Letters, 2004 , vol. 6, # 14 p. 2457 - 2460
反应条件
tetrachloromethane; sulfur dioxide; iodine; acetic acid
T=170 - 235°C; weiteres Reagens: rauchende Salpetersaeure;
参考文献
Varma; Raman
Journal of the Indian Chemical Society, 1935 , vol. 12, p. 343
反应条件
sulfuric acid; iodine; oxygen; nitric acid in water
T=49.9°C; P=750.06 Torr; 1 h; Rate constant;
参考文献
Dorfman; Aleshkova
Russian Journal of Organic Chemistry, 1997 , vol. 33, # 11 p. 1585 - 1597
反应条件
T=170 - 235°C; weitere Verbindung: rauchende Salpetersaeure;
参考文献
Varma; Raman
Journal of the Indian Chemical Society, 1935 , vol. 12, p. 245,247
参考文献
Varma; Sreenivasmurthyachar
Journal of the Indian Chemical Society, 1936 , vol. 13, p. 187
Full Text Show Details
Varma; Raman
Journal of the Indian Chemical Society, 1935 , vol. 12, p. 343