3H-2-氧杂-1H-非那烯-1-酮合成路线 （共 20 条）
反应条件
potassium hydroxide; formaldehyd
参考文献
Fuson; Munn
Journal of the American Chemical Society, 1949 , vol. 71, p. 1870
反应条件
1: sodium tetrahydroborate / methanol / 0 - 20 °C
2: aluminum oxide; potassium meta-periodate / 0.17 h / Microwave irradiation
View Scheme
参考文献
Dakdouki, Saada C.; Villemin, Didier; Bar, Nathalie
European Journal of Organic Chemistry, 2011 , # 23 p. 4448 - 4454
反应条件
aluminum oxide; potassium meta-periodate
0.166667 h; Microwave irradiation;
参考文献
Dakdouki, Saada C.; Villemin, Didier; Bar, Nathalie
European Journal of Organic Chemistry, 2011 , # 23 p. 4448 - 4454
反应条件
potassium permanganate; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane
6 h; Heating;
参考文献
Markgraf, J. Hodge; Choi, Bo Yoon
Synthetic Communications, 1999 , vol. 29, # 14 p. 2405 - 2411
反应条件
oxygen; Manganese (II) acetate in various solvent(s)
T=100 - 140°C; 2 h;
参考文献
Tkacheva, G. D.; Suvorov, B. V.
Journal of Organic Chemistry USSR (English Translation), 1985 , p. 1173 - 1177
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 6 p. 1289 - 1293
反应条件
Cu(OAc)2*2H2O; Mn(II)(OAc)2*2H2O; oxygen; acetic acid; potassium bromide
T=105°C;
参考文献
Bukharkina, Tatiana V.; Grechishkina, Olga S.; Digurov, Nikolai G.; Kon'kov, Ivan I.
Organic Process Research and Development, 2002 , vol. 6, # 4 p. 394 - 400
反应条件
lithium aluminium tetrahydride; zinc(II) chloride in tetrahydrofuran
T=0 - 20°C; Product distribution; Further Variations:ReagentsTemperatures;
参考文献
Luo, Huan; Zeng, Qingle; Liu, Zhongrong; Wei, Yongzhi; Li, Bogang; Wang, Fengpeng
Synthetic Communications, 2004 , vol. 34, # 12 p. 2269 - 2275
反应条件
Cu(OAc)2*2H2O; Mn(II)(OAc)2*2H2O; oxygen; acetic acid; potassium bromide
3.33333 h; Heating;
参考文献
Bukharkina, Tatiana V.; Grechishkina, Olga S.; Digurov, Nikolai G.; Kon'kov, Ivan I.
Organic Process Research and Development, 2002 , vol. 6, # 4 p. 394 - 400
反应条件
Cannizzaro reaction;
参考文献
Dakdouki, Saada C.; Villemin, Didier; Bar, Nathalie
European Journal of Organic Chemistry, 2011 , # 23 p. 4448 - 4454
参考文献
Fuson; Munn
Journal of the American Chemical Society, 1949 , vol. 71, p. 1870
