反应条件
2: 86 percent / thionyl chloride / methanol / 6 h / Heating
3: 88 percent / lithium aluminum hydride / diethyl ether / 5 h / Heating
4: 1.) N-chlorosuccinimide, dimethyl sulfide, 2.) triethylamine / 1.) tolueene, - 25 deg C, 2.5 h, 2.) -25 deg C -> 25 deg C; other reagents
5: 94 percent / hydrochloric acid / aq. ethanol
6: 1.) sodium hydride / 1.) dichloromethane, 2.) chlorobenzene, 120 deg C, 0.5 h
7: lithium aluminum hydride / diethyl ether / Ambient temperature
View Scheme
参考文献
Bailey, R. J.; Card, P. J.; Shechter, H.
Journal of the American Chemical Society, 1983 , vol. 105, # 19 p. 6096 - 6103
