Cho, Won Seok; Kim, So Han; Kim, Da Jung; Mun, Sang-Deok; Kim, Ran; Go, Min Jeong; Park, Myung Hwan; Kim, Min; Lee, Junseong; Kim, Youngjo
Polyhedron, 2014 , vol. 67, p. 205 - 212
di-isopropyl azodicarboxylate; triphenylphosphine in tetrahydrofuran
T=0 - 20°C; Inert atmosphere;
参考文献
Murphy, John A.; Schoenebeck, Franziska; Findlay, Neil J.; Thomson, Douglas W.; Zhou, Sheng-ze; Garnier, Jean
Journal of the American Chemical Society, 2009 , vol. 131, p. 6475 - 6479
1.1: sodium hydroxide / water / 0.17 h / |Reflux; |Inert atmosphere
1.2: 40 h / |Reflux; |Inert atmosphere; |Glovebox
2.1: triethylamine / dichloromethane / 0.17 h / 0 °C / |Inert atmosphere; |Schlenk technique; |Glovebox
2.2: 3 h / 0 - 20 °C / |Inert atmosphere; |Schlenk technique; |Glovebox
3.1: lithium bromide / acetone / 24 h / 20 °C
View Scheme
参考文献
Cho, Won Seok; Kim, So Han; Kim, Da Jung; Mun, Sang-Deok; Kim, Ran; Go, Min Jeong; Park, Myung Hwan; Kim, Min; Lee, Junseong; Kim, Youngjo
Polyhedron, 2014 , vol. 67, p. 205 - 212
