反应条件
1: di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; O,O’-(S)-1,1’-(dinaphthyl-2,2’-diyl)-N,N’-di-(S,S)-1-(2-methoxyphenyl)ethylphosphoramidite; 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 5 h / 50 °C / Inert atmosphere 2: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere 3: sodium periodate; ruthenium trichloride / tetrachloromethane; water; acetonitrile / 20 °C / Inert atmosphere View Scheme
参考文献
Xia, Jibao; Zhuo, Chunxiang; You, Shuli
Chinese Journal of Chemistry, 2010 , vol. 28, # 9 p. 1525 - 1528