反应条件
1: 70 percent / NaH, 1,3-diaminopropane / 1) 10 deg C, 2) 100 deg C, 40 min
2: 81.8 percent / (diethylamino)sulfur trifluoride / CH2Cl2 / 1) -78 deg C, 2) room temperature
3: 1) n-butyllithium / 1) THF/HMPA, 0 deg C - room temperature , 2) THF, 0 deg C, 1 h
4: 91 percent / H2, quinoline / Pd/BaSO4 / methanol
View Scheme
参考文献
Carvalho, Joan F.; Prestwich, Glenn D.
Journal of Organic Chemistry, 1984 , vol. 49, # 7 p. 1251 - 1258
