1-氯-4-(苯基乙炔基)苯合成路线 （共 58 条）
反应条件
C41H38BFeN3P2; hydrogen in tetrahydrofuran T=20 - 90°C; P=7500.75 Torr; 23 h; Inert atmosphere;
参考文献
Srimani, Dipankar; Diskin-Posner, Yael; Ben-David, Yehoshoa; Milstein, David
Angewandte Chemie - International Edition, 2013 , vol. 52, # 52 p. 14131 - 14134
Angew. Chem., 2013 , vol. 125, # 52 p. 14381 - 14383
反应条件
water; copper; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in acetonitrile T=20°C; 4 h;
参考文献
Zhang, Wenxia; Zhang, Jian; Liu, Yunkui; Xu, Zhenyuan
Synlett, 2013 , vol. 24, # 20 art. no. ST-2013-W0765-L, p. 2709 - 2714
反应条件
anhydrous lithium nitrate in water; acetonitrile Electrochemical reaction;
参考文献
Australian Journal of Chemistry, , vol. 60, # 6 p. 420 - 428
反应条件
(5,10,15,20-tetraphenylporphyrinato)manganese(III) chloride; oxygen in hexane T=150°C; P=15001.5 Torr; 4 h;
参考文献
Sheng, Wen-Bing; Jiang, Qing; Luo, Wei-Ping; Guo, Can-Cheng
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5691 - 5693
反应条件
anhydrous lithium nitrate in water; acetonitrile Electrochemical reaction;
参考文献
Australian Journal of Chemistry, , vol. 60, # 6 p. 420 - 428
反应条件
lithium hydroxide hydrate; C24H23N3O3PdS in N,N-dimethyl-formamide T=130°C; Larock Annulation; 24 h; Overall yield = 82 percent; regioselective reaction;
参考文献
Srinivas, Keesara; Saiprathima, Parvathaneni; Balaswamy, Kodicherla; Ra, Mandapati Mohan
Journal of Organometallic Chemistry, 2013 , vol. 741-742, # 1 p. 162 - 167
反应条件
lithium hydroxide hydrate; C24H23N3O3PdS in N,N-dimethyl-formamide T=130°C; Larock Annulation; 24 h; Overall yield = 82 percent; regioselective reaction;
参考文献
Srinivas, Keesara; Saiprathima, Parvathaneni; Balaswamy, Kodicherla; Ra, Mandapati Mohan
Journal of Organometallic Chemistry, 2013 , vol. 741-742, # 1 p. 162 - 167
反应条件
tetrabutylammomium bromide; [1-cyclohexyl-3-(di-pyridin-2-yl-methyl)-urea][PdCl2] in 1-methyl-pyrrolidin-2-one
T=110°C; 0.25 h;
参考文献
Gil-Molto, Juan; Najera, Carmen
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 14 p. 1874 - 1882
反应条件
copper(l) iodide; potassium carbonate; triphenylphosphine in dimethyl sulfoxide
T=90°C; 24 h; Inert atmosphere;
参考文献
Qu, Xiaoming; Li, Tingyi; Sun, Peng; Zhu, Yan; Yang, Hailong; Mao, Jincheng
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 20 p. 6938 - 6942
反应条件
pyrrolidine; tetrabutylammomium bromide; PdCl2 (dipyridin-2-yl)methylamine complex in water
T=100°C; Sonogashira coupling; P=750.075 Torr; 1 h;
参考文献
Kawanami, Hajime; Matsushima, Keiichiro; Sato, Masahiro; Ikushima, Yutaka
Angewandte Chemie - International Edition, 2007 , vol. 46, # 27 p. 5129 - 5132
