2,6-二溴-4-甲基苯甲醚合成路线 （共 7 条）
反应条件
copper(l) chloride in methanol; N,N-dimethyl-formamide T=140°C; 8 h; Autoclave; TemperatureTime;
参考文献
Sankaranarayanan, Ananthakrishnan; Chandalia
Organic Process Research and Development, 2006 , vol. 10, # 3 p. 487 - 492
反应条件
copper(l) chloride in methanol; N,N-dimethyl-formamide T=70 - 105°C; 7 h;
参考文献
Sankaranarayanan, Ananthakrishnan; Chandalia
Organic Process Research and Development, 2006 , vol. 10, # 3 p. 487 - 492
反应条件
copper(l) chloride in methanol; N,N-dimethyl-formamide T=140°C; 8 h; Autoclave; TemperatureTime;
参考文献
Sankaranarayanan, Ananthakrishnan; Chandalia
Organic Process Research and Development, 2006 , vol. 10, # 3 p. 487 - 492
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 37 h / |Inert atmosphere; |Reflux 2: potassium carbonate / methanol / 20 °C 3: acetic acid; palladium 10 on activated carbon; sodium tetrahydroborate / isopropyl alcohol / 1.5 h / 20 °C 4: boron tribromide / dichloromethane / 18.5 h / 0 - 20 °C View Scheme
参考文献
Zhao, Wenjun; Huang, Li; Guan, Yong; Wulff, William D.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 13 p. 3436 - 3441
Angew. Chem., 2014 , vol. 126, # 13 p. 3504 - 3509,6
反应条件
boron tribromide; triphenylphosphine; palladium diacetate in ethylene glycol dimethyl ether; hexane; dichloromethane; water
参考文献
SK Energy Co., Ltd.
Patent: US2009/326175 A1, 2009 ;
反应条件
copper(l) chloride in methanol; N,N-dimethyl-formamide
T=140°C; 8 h; Autoclave; TemperatureTime;
参考文献
Sankaranarayanan, Ananthakrishnan; Chandalia
Organic Process Research and Development, 2006 , vol. 10, # 3 p. 487 - 492
反应条件
boron tribromide; triphenylphosphine; palladium diacetate in ethylene glycol dimethyl ether; hexane; dichloromethane; water
参考文献
SK Energy Co., Ltd.
Patent: US2009/326175 A1, 2009 ;
