zinc T=30 - 35°C;

SbF5 T=50°C; 0.5 h;

lithium bromide in diethylene glycol dimethyl ether T=25°C; 1 h;

lithium chloride in diethylene glycol dimethyl ether T=25°C; 0.5 h;

cesium fluoride in diethylene glycol dimethyl ether T=-196 - 25°C; 3.5 h; AutoclaveInert atmosphere;

1: α-(fluorosulfato)pentafluoroacetone With KHF2 in nitrobenzene T=45 - 60°C; P=100 Torr; 2: With cesium fluoride in diethylene glycol dimethyl ether; bis [2-(2-methoxyethoxy)ethyl] ether T=-32 - -30°C; 0.5 h; 3: hexafluorocyclopropylene oxide in diethylene glycol dimethyl ether; bis [2-(2-methoxyethoxy)ethyl] ether T=-32 - -30°C; 2.5 h;

cesium fluoride in diethylene glycol dimethyl ether T=-35 - 20°C; 3.5 h;

1: α-(fluorosulfato)pentafluoroacetone With KHF2 in nitrobenzene T=45 - 60°C; P=100 Torr; 2: With cesium fluoride in diethylene glycol dimethyl ether; bis [2-(2-methoxyethoxy)ethyl] ether T=-32 - -30°C; 0.5 h; 3: hexafluorocyclopropylene oxide in diethylene glycol dimethyl ether; bis [2-(2-methoxyethoxy)ethyl] ether T=-32 - -30°C; 2.5 h;

in various solvent(s) T=100 - 140°C; Irradiationother α-ketofluorosulfates; other temperatures and solvents; Product distribution;