1-(2-硝基苯基)-1,2-乙二醇合成路线 （共 15 条）
反应条件
[bis(acetoxy)iodo]benzene in dichloromethane T=25°C; 8 h; Inert atmosphere;
参考文献
Nicolaou; Adsool, Vikrant A.; Hale, Christopher R. H.
Organic Letters, 2010 , vol. 12, # 7 p. 1552 - 1555
反应条件
toluene-4-sulfonic acid in benzene
参考文献
E. I. Du Pont de Nemours and Company
Patent: US4111960 A1, 1978 ;
反应条件
toluene-4-sulfonic acid in acetone
参考文献
E. I. Du Pont de Nemours and Company
Patent: US4111960 A1, 1978 ;
反应条件
toluene-4-sulfonic acid in benzene
1 h; in the dark;
参考文献
Gravel, D.; Herbert, J.; Thoraval, D.
Canadian Journal of Chemistry, 1983 , vol. 61, p. 400 - 410
反应条件
toluene-4-sulfonic acid in benzene
2 h; Heating;
参考文献
Ceita, Luisa; Maiti, Amiya K.; Mestres, Ramon; Tortajada, Amparo
Journal of Chemical Research, Miniprint, 2001 , # 10 p. 1023 - 1055
反应条件
potassium carbonate in aqueous 1,4-dioxane
参考文献
National Research Development Corporation
Patent: US4657926 A1, 1987 ;
反应条件
dihydrogen peroxide; ethyl acetate; lipase [PSLG6] in water
T=60°C; 0.116667 h; microwave irradiation;
参考文献
Sarma, Kuladip; Borthakur, Naleen; Goswami, Amrit
Tetrahedron Letters, 2007 , vol. 48, # 38 p. 6776 - 6778
反应条件
potassium carbonate in 1,4-dioxane
17 h; Heatingin the dark;
参考文献
Gravel, D.; Herbert, J.; Thoraval, D.
Canadian Journal of Chemistry, 1983 , vol. 61, p. 400 - 410
反应条件
perchloric acid in tetrahydrofuran
20 h; Ambient temperature;
参考文献
Wierenga, Wendell; Harrison, Allen W.; Evans, Bruce R.; Chidester, Connie G.
Journal of Organic Chemistry, 1984 , vol. 49, # 3 p. 438 - 442
反应条件
1: 68 percent / bromine / dioxane / 2 h
2: 88 percent / sodium borohydride / dioxane; H2O / 1.) 2 h at 5 deg C; 2.) 30 min room temperature
3: 78 percent / 10 percent aq potassium carbonate / dioxane / 17 h / Heating; in the dark
View Scheme
参考文献
Gravel, D.; Herbert, J.; Thoraval, D.
Canadian Journal of Chemistry, 1983 , vol. 61, p. 400 - 410
