5-溴-4-(噻吩-2-基)嘧啶合成路线 （共 5 条）
反应条件
palladium diacetate; potassium carbonate; tri-cyclo-hexyl-phosphine in trifluoroacetic acid
T=20°C; 0.166667 h; Inert atmosphereMicrowave irradiation;
参考文献
Verbitskiy, Egor V.; Cheprakova, Ekaterina M.; Zhilina, Ekaterina F.; Kodess, Mikhail I.; Ezhikova, Marina A.; Pervova, Marina G.; Slepukhin, Pavel A.; Subbotina, Julia O.; Schepochkin, Aleksandr V.; Rusinov, Gennady L.; Chupakhin, Oleg N.; Charushin, Valery N.
Tetrahedron, 2013 , vol. 69, # 25 p. 5164 - 5172
反应条件
palladium diacetate; potassium carbonate; tri-cyclo-hexyl-phosphine in trifluoroacetic acid
T=20°C; 0.166667 h; Inert atmosphereMicrowave irradiation;
参考文献
Verbitskiy, Egor V.; Cheprakova, Ekaterina M.; Zhilina, Ekaterina F.; Kodess, Mikhail I.; Ezhikova, Marina A.; Pervova, Marina G.; Slepukhin, Pavel A.; Subbotina, Julia O.; Schepochkin, Aleksandr V.; Rusinov, Gennady L.; Chupakhin, Oleg N.; Charushin, Valery N.
Tetrahedron, 2013 , vol. 69, # 25 p. 5164 - 5172
反应条件
potassium hydroxide; potassium hexacyanoferrate(III) in water
2 h;
参考文献
Verbitskiy, Egor V.; Cheprakova, Ekaterina M.; Slepukhin, Pavel A.; Kodess, Mikhail I.; Ezhikova, Marina A.; Pervova, Marina G.; Rusinov, Gennady L.; Chupakhin, Oleg N.; Charushin, Valery N.
Tetrahedron, 2012 , vol. 68, # 27-28 p. 5445 - 5452
反应条件
diethylamine
T=20°C; 24 h;
参考文献
Verbitskiy, Egor V.; Cheprakova, Ekaterina M.; Slepukhin, Pavel A.; Kodess, Mikhail I.; Ezhikova, Marina A.; Pervova, Marina G.; Rusinov, Gennady L.; Chupakhin, Oleg N.; Charushin, Valery N.
Tetrahedron, 2012 , vol. 68, # 27-28 p. 5445 - 5452
反应条件
(i) nBuLi, Et2O, (ii) /BRN= 107326/, (iii) KMnO4; Multistep reaction;
参考文献
Gronowitz,S.; Roee,J.
Acta Chemica Scandinavica (1947-1973), 1965 , vol. 19, p. 1741 - 1748
