N-亚苄基-4-甲基苯磺酰胺合成路线 （共 129 条）
反应条件
potassium tert-butylate in tert-butyl alcohol T=50°C;
参考文献
Journal of Organic Chemistry, , vol. 72, # 15 p. 5905 - 5907
反应条件
1: 18 percent / t-BuOK / 2-methyl-propan-2-ol / 50 °C 2: 85 percent / t-BuOK / 2-methyl-propan-2-ol / 50 °C View Scheme
参考文献
Fan, Renhua; Wang, Weizi; Pu, Dongming; Wu, Jie
Journal of Organic Chemistry, 2007 , vol. 72, # 15 p. 5905 - 5907
反应条件
1: N-benzylidene-4-methylbenzenesulfonamide; Cr(CO)3*PhCHO With samarium diiodide in tetrahydrofuran T=0 - 20°C; 2: acetic anhydride With pyridine 3: With air Irradiation; Further stages.;
参考文献
Tanaka, Yoshie; Taniguchi, Nobukazu; Kimura, Takayuki; Uemura, Motokazu
Journal of Organic Chemistry, 2002 , vol. 67, # 26 p. 9227 - 9237
反应条件
1: N-benzylidene-4-methylbenzenesulfonamide; Cr(CO)3*PhCHO With samarium diiodide in tetrahydrofuran T=0 - 20°C; 2: acetic anhydride With pyridine 3: With air Irradiation; Further stages.;
参考文献
Tanaka, Yoshie; Taniguchi, Nobukazu; Kimura, Takayuki; Uemura, Motokazu
Journal of Organic Chemistry, 2002 , vol. 67, # 26 p. 9227 - 9237
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 0.08 h / -40 °C 1.2: 67 percent / tetrahydrofuran; hexane / 2 h / -40 - -20 °C 2.1: 73 percent / O3 / -78 °C View Scheme
参考文献
Amombo, Marlyse Okala; Hausherr, Arndt; Reissig, Hans-Ulrich
Synlett, 1999 , # 12 p. 1871 - 1874
反应条件
1: 82 percent / Zn-Cu / tetrahydrofuran / Heating 2: 76 percent / TFA / 2 h / 20 °C 3: sodium, naphthalene / 1,2-dimethoxy-ethane View Scheme
参考文献
Robinson, Andrew J.; Wyatt, Peter B.
Tetrahedron, 1993 , vol. 49, # 48 p. 11329 - 11340
反应条件
indium in methanol; water T=20°C; 1 h;
参考文献
Organic Letters, , vol. 4, # 1 p. 131 - 133
反应条件
H218O in acetonitrile T=20°C; 24 h; Inert atmosphere;
参考文献
European Journal of Organic Chemistry, , # 6 p. 1084 - 1091
反应条件
triethyl borane; sodium hydroxide in hexane; dichloromethane T=-78°C; 10 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 77, # 3 p. 1547 - 1553
反应条件
sodium hydride in tetrahydrofuran T=24°C; 25 h;
参考文献
Baird, Charlotte P.; Taylor, Paul C.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 20 p. 3399 - 3403
