N-亚苄基-4-甲基苯磺酰胺合成路线 （共 129 条）
反应条件
in dimethyl sulfoxide T=100°C; 12 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Fang, Fan; Li, Yuan; Tian, Shi-Kai
European Journal of Organic Chemistry, 2011 , # 6 p. 1084 - 1091
反应条件
4 A molecular sieve; i-Pr2NPPh2; potassium carbonate; bis(benzonitrile)palladium(II) dichloride in 1,4-dioxane T=80°C; Suzuki reaction; 24 h;
参考文献
Zhang, Qiang; Chen, Jiuxi; Liu, Miaochang; Wu, Huayue; Cheng, Jiang; Qin, Changming; Su, Weike; Ding, Jinchang
Synlett, 2008 , # 6 p. 935 - 939
反应条件
potassium fluoride; [Rh(NCMe)2(cod)][BF4] in N,N-dimethyl-formamide T=60°C; 20 h;
参考文献
Oi, Shuichi; Moro, Mitsutoshi; Kawanishi, Takanori; Inoue, Yoshio
Tetrahedron Letters, 2004 , vol. 45, # 25 p. 4855 - 4857
反应条件
chloro-trimethyl-silane; bismuth sulphate in dichloromethane T=20°C; Friedel-Crafts reaction; 4 h;
参考文献
Liu, Cong-Rong; Li, Man-Bo; Yang, Cui-Feng; Tian, Shi-Kai
Chemical Communications, 2008 , # 10 p. 1249 - 1251
反应条件
in dimethyl sulfoxide T=100°C; 12 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Fang, Fan; Li, Yuan; Tian, Shi-Kai
European Journal of Organic Chemistry, 2011 , # 6 p. 1084 - 1091
反应条件
1.1: potassium tert-butylate / methanol / 4 h / 20 °C / Inert atmosphere 1.2: 36 h / 70 °C 2.1: methanol; potassium hydroxide / 72 h / Reflux; Inert atmosphere View Scheme
参考文献
Barber, David M.; Sanganee, Hitesh; Dixon, Darren J.
Chemical Communications, 2011 , vol. 47, # 15 p. 4379 - 4381
反应条件
dimethyl sulfoxide T=20°C; Knoevenagel condensation; 2 h; Inert atmosphereMolecular sieve; stereoselective reaction;
参考文献
Chiba, Ryoichi; Oriyama, Takeshi
Chemistry Letters, 2008 , vol. 37, # 12 p. 1218 - 1219
反应条件
water; diisopropylamine in DMF-d7 T=-78°C; Substitution; Mannich-type reaction; Addition; 18 h; Title compound not separated from byproducts;
参考文献
Miura, Katsukiyo; Tamaki, Kentaro; Nakagawa, Takahiro; Hosomi, Akira
Angewandte Chemie - International Edition, 2000 , vol. 39, # 11 p. 1958 - 1960
反应条件
1: N-benzylidene-4-methylbenzenesulfonamide; Cr(CO)3*PhCHO With samarium diiodide in tetrahydrofuran T=0 - 20°C; 2: acetic anhydride With pyridine 3: With air Irradiation; Further stages.;
参考文献
Tanaka, Yoshie; Taniguchi, Nobukazu; Kimura, Takayuki; Uemura, Motokazu
Journal of Organic Chemistry, 2002 , vol. 67, # 26 p. 9227 - 9237
反应条件
[bis(acetoxy)iodo]benzene; potassium tert-butylate; tetrabutylammomium bromide in acetonitrile T=0 - 30°C; ReactivityMechanism; Reagent/catalystSolvent;
参考文献
Fan, Renhua; Ye, Yang
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 10 p. 1526 - 1530
