N,N-二甲基-4-丙-2-烯基-苯胺合成路线 (共 17 条)
反应条件
bis(η3-allyl-μ-chloropalladium(II)) in ethylene glycol dimethyl ether T=85°C; 7 h; Inert atmosphere;
参考文献
Denmark, Scott E.; Werner, Nathan S.
Journal of the American Chemical Society, 2008 , vol. 130, # 48 p. 16382 - 16393
反应条件
xanthone powder in acetonitrile T=20°C; Photolysis;
参考文献
Milanesi, Silvia; Fagnoni, Maurizio; Albini, Angelo
Chemical Communications, 2003 , # 2 p. 216 - 217
反应条件
1: 4-iodo-N,N-dimethylaniline With tBu4ZnLi2 in tetrahydrofuran T=-78 - 0°C; Inert atmosphere; 2: allyl bromide in tetrahydrofuran T=20°C; 12 h; Inert atmosphere; chemoselective reaction;
参考文献
Furayama, Taniyuki; Yonehara, Mitsuhiro; Arimoto, Sho; Kobayashi, Minoru; Matsumoto, Yotaro; Uchiyama, Masanobu
Chemistry - A European Journal, 2008 , vol. 14, # 33 p. 10348 - 10356
反应条件
1: 4-bromo-N,N-dimethyl-aniline With magnesium; lithium chloride in tetrahydrofuran T=20°C; 2 h; Inert atmosphere; 2: With iron (III) acetylacetonate in tetrahydrofuran T=0°C; 0.0833333 h; Inert atmosphere; 3: ethylene,methyl acetate in tetrahydrofuran T=0°C; 0.75 h; Inert atmosphere;
参考文献
Mayer, Matthias; Czaplik, Waldemar M.; Von Wangelin, Axel Jacobi
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 13 p. 2147 - 2152
反应条件
in acetonitrile ionic Meerwein arylation; Irradiation;
参考文献
Dichiarante, Valentina; Betti, Cecilia; Fagnoni, Maurizio; Maia, Angelamaria; Landini, Dario; Albini, Angelo
Chemistry - A European Journal, 2007 , vol. 13, # 6 p. 1834 - 1841
反应条件
triethylamine in 2,2,2-trifluoroethanol 4 h; Photolysis;
参考文献
De Carolis, Marco; Protti, Stefano; Fagnoni, Maurizio; Albini, Angelo
Angewandte Chemie - International Edition, 2005 , vol. 44, # 8 p. 1232 - 1236
反应条件
triethylamine in 2,2,2-trifluoroethanol 5 h; Photolysis;
参考文献
De Carolis, Marco; Protti, Stefano; Fagnoni, Maurizio; Albini, Angelo
Angewandte Chemie - International Edition, 2005 , vol. 44, # 8 p. 1232 - 1236
反应条件
triethylamine in 2,2,2-trifluoroethanol Photolysis;
参考文献
De Carolis, Marco; Protti, Stefano; Fagnoni, Maurizio; Albini, Angelo
Angewandte Chemie - International Edition, 2005 , vol. 44, # 8 p. 1232 - 1236
反应条件
caesium carbonate in 2,2,2-trifluoroethanol 6 h; UV-irradiation;
参考文献
Dichiarante, Valentina; Salvaneschi, Andrea; Protti, Stefano; Dondi, Daniele; Fagnoni, Maurizio; Albini, Angelo
Journal of the American Chemical Society, 2007 , vol. 129, # 51 p. 15919 - 15926
反应条件
in acetonitrile Irradiation;
参考文献
Fagnoni, Maurizio; Mella, Mariella; Albini, Angelo
Organic Letters, 1999 , vol. 1, # 8 p. 1299 - 1301