in tetrahydrofuran
LiNMe2/complex=1.5 (Ar, room temp., 2 h), then addn. of (MeO)2SO2, stirring (30 min, 25°C); not isolated, detd. by gas chromy.;
参考文献
Kawasaki, Nobuo; Masuzoe, Kenji; Ozawa, Fumiyuki; Yamamoto, Akio
Journal of Organometallic Chemistry, 1989 , vol. 361, p. C37 - C40
→
反应条件
carbon monoxide; acetone in acetone
byproducts: dimethylamine; treatment of trans-Pd(COPh)(CONMe2)(PMe3)2 with Me2NH2BF4 (1 equiv.) in acetone under CO;
参考文献
Ozawa, Fumiyuki; Huang, Li; Yamamoto, Akio
Journal of Organometallic Chemistry, 1987 , vol. 334, p. C9 - C13