1,4-二碘-2,5-二甲氧基苯合成路线 （共 24 条）
反应条件
sulfuric acid; iodine; iodic acid; acetic acid in tetrachloromethane; water 24 h; Heating;
参考文献
Yamaguchi, Yoshihiro; Kobayashi, Shigeya; Wakamiya, Tateaki; Matsubara, Yoshio; Yoshida, Zen-Ichi
Angewandte Chemie - International Edition, 2005 , vol. 44, # 43 p. 7040 - 7044
反应条件
[I(py)2]BF4; trifluorormethanesulfonic acid in dichloromethane T=20°C; 3 h;
参考文献
Lopez-Alvarado, Pilar; Avendano, Carmen; Menendez, J. Carlos
Synthetic Communications, 2002 , vol. 32, # 20 p. 3233 - 3239
反应条件
1: iodine; AcOH; sulfuric acid / CCl4 2: NaOH / H2O; 2-methyl-propan-2-ol 3: K2CO3 / acetone 4: 76 percent / iodine; iodic acid; sulfuric acid / acetic acid / H2O; CCl4 / 24 h / Heating View Scheme
参考文献
Yamaguchi, Yoshihiro; Kobayashi, Shigeya; Wakamiya, Tateaki; Matsubara, Yoshio; Yoshida, Zen-Ichi
Angewandte Chemie - International Edition, 2005 , vol. 44, # 43 p. 7040 - 7044
反应条件
1: K2CO3 / acetone 2: 76 percent / iodine; iodic acid; sulfuric acid / acetic acid / H2O; CCl4 / 24 h / Heating View Scheme
参考文献
Yamaguchi, Yoshihiro; Kobayashi, Shigeya; Wakamiya, Tateaki; Matsubara, Yoshio; Yoshida, Zen-Ichi
Angewandte Chemie - International Edition, 2005 , vol. 44, # 43 p. 7040 - 7044
反应条件
1: NaOH / H2O; 2-methyl-propan-2-ol 2: K2CO3 / acetone 3: 76 percent / iodine; iodic acid; sulfuric acid / acetic acid / H2O; CCl4 / 24 h / Heating View Scheme
参考文献
Yamaguchi, Yoshihiro; Kobayashi, Shigeya; Wakamiya, Tateaki; Matsubara, Yoshio; Yoshida, Zen-Ichi
Angewandte Chemie - International Edition, 2005 , vol. 44, # 43 p. 7040 - 7044
反应条件
iodine cloride in water; acetic acid
参考文献
The Regents of the University of California
Patent: US4647446 A1, 1987 ;
反应条件
iodine cloride in acetonitrile T=70°C; 4 h;
参考文献
Wariishi, Koji; Morishima, Sin-Ichi; Inagaki, Yoshio
Organic Process Research and Development, 2003 , vol. 7, # 1 p. 98 - 100
反应条件
iodine cloride in acetic acid T=70°C; 4 h;
参考文献
Wariishi, Koji; Morishima, Sin-Ichi; Inagaki, Yoshio
Organic Process Research and Development, 2003 , vol. 7, # 1 p. 98 - 100
反应条件
sulfuric acid; iodine in acetonitrile T=0°C; 0.5 h; ElectrolysisFlow reactor; regioselective reaction;
参考文献
Midorikawa, Koji; Suga, Seiji; Yoshida, Jun-Ichi
Chemical Communications, 2006 , # 36 p. 3794 - 3796
反应条件
1: 1.) NaNO2, HCl, 2.) KI 2: ICl / CH2Cl2 / 22 h / 25 °C View Scheme
参考文献
Hubig, S. M.; Jung, W.; Kochi, J. K.
Journal of Organic Chemistry, 1994 , vol. 59, # 21 p. 6233 - 6244
