1,2:4,5-双-o-(1-甲基亚乙基)-muco-肌醇合成路线 （共 9 条）
反应条件
1: 91 percent / NaH / dimethylformamide / 2 h / Ambient temperature 2: 80 percent / PTSA, ethane-1,2-diol, Et3N / CH2Cl2 / Ambient temperature View Scheme
参考文献
Gigg, Jill; Gigg, Roy; Payne, Sheila; Conant, Robert
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 423 - 430
反应条件
palladium dihydroxide in methanol 88 h; Heating;
参考文献
Murali, Chebrolu; Shashidhar, Mysore S.; Gopinath, Chinnakonda S.
Tetrahedron, 2007 , vol. 63, # 19 p. 4149 - 4155
反应条件
1: pyridine / 0 °C 2: 100 percent / isobutylamine / methanol / Heating 3: 6 percent / pyridine / CH2Cl2 / -20 °C 4: 100 percent / N,N-dimethyl-acetamide / 70 °C 5: 100 percent / NaOMe / methanol / Heating 6: aq. TFA / 20 °C View Scheme
参考文献
Sureshan, Kana M.; Watanabe, Yutaka
Synlett, 2004 , # 3 p. 493 - 496
反应条件
1H-imidazole in pyridine T=-20°C; 48 h;
参考文献
Rukavishnikov, Aleksey V.; O. Zaikova, Tatiana; Griffith, O. Hayes; Keana, John F.W.
Chemistry and Physics of Lipids, 1997 , vol. 89, # 2 p. 153 - 157
反应条件
1: 1.) NaH / DMF, 25 deg C
2: 99 percent / DBU / dimethylformamide / 60 °C
3: 98 percent / H2 / Pd(OH)2 / ethanol; triethylamine / 25 °C / 2585.7 Torr
View Scheme
参考文献
Kulagowski, Janusz J.
Tetrahedron Letters, 1989 , vol. 30, # 29 p. 3869 - 3872
反应条件
sodium hydride in toluene
12 h; Heating;
参考文献
Chung, Sung-Kee; Ryu, Youngha
Carbohydrate Research, 1994 , vol. 258, p. 145 - 168
反应条件
sodium hydride in N,N-dimethyl-formamide
2 h; Ambient temperature;
参考文献
Mills, Stephen J.; Potter, Barry V. L.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 9 p. 1279 - 1286
反应条件
sodium hydride in N,N-dimethyl-formamide
12 h; Ambient temperature;
参考文献
Chung, Sung-Kee; Ryu, Youngha
Carbohydrate Research, 1994 , vol. 258, p. 145 - 168
参考文献
Gigg, Jill; Gigg, Roy; Payne, Sheila; Conant, Robert
Carbohydrate Research, 1985 , vol. 140, p. C1 - C3
