(2E)-2-十四碳烯醛合成路线 （共 11 条）
反应条件
in toluene
19 h; Reflux;
参考文献
Okutani, Masaru; Mori, Yuji
Journal of Organic Chemistry, 2009 , vol. 74, # 1 p. 442 - 444
反应条件
pyridinium chlorochromate in dichloromethane
参考文献
Kirin Beer Kabushiki Kaisha
Patent: US5461036 A1, 1995 ;
反应条件
N-chloro-succinimide; PhSNH-t-Bu; 1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane
T=0°C; 1 h;
参考文献
Seo, Seon-M.I.; Junheon, Kim; Eunae, Kim; Park, Hye-M.I.; Kim, Young-Joon; Park, I.L.-Kwon
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 3 p. 1823 - 1827
反应条件
sodium hydrogencarbonate in tetrahydrofuran; water
4 h; Heating;
参考文献
Pohmakotr, Manat; Pisutjaroenpong, Somchai
Tetrahedron Letters, 1985 , vol. 26, # 30 p. 3613 - 3616
反应条件
1: 67 percent / lithium diisopropylamide, hexamethylphosphortriamide / tetrahydrofuran / -78 °C
2: tetrafluoroboric acid (50percent) / CH2Cl2; H2O / 7 h / Heating
3: 70 percent / NaHCO3 / tetrahydrofuran; H2O / 4 h / Heating
View Scheme
参考文献
Pohmakotr, Manat; Pisutjaroenpong, Somchai
Tetrahedron Letters, 1985 , vol. 26, # 30 p. 3613 - 3616
反应条件
1: tetrafluoroboric acid (50percent) / CH2Cl2; H2O / 7 h / Heating
2: 70 percent / NaHCO3 / tetrahydrofuran; H2O / 4 h / Heating
View Scheme
参考文献
Pohmakotr, Manat; Pisutjaroenpong, Somchai
Tetrahedron Letters, 1985 , vol. 26, # 30 p. 3613 - 3616
反应条件
mercury dichloride in tetrahydrofuran; acetonitrile
参考文献
Stoffel; Melzner
1973 , vol. 354, # 12 p. 1626 - 1632
参考文献
Wailes
Australian Journal of Chemistry, 1959 , vol. 12, p. 173,186
反应条件
1: Lindlar-catalyst; quinoline; methyl acetate / Hydrogenation
2: aqueous sulfuric acid
View Scheme
参考文献
Wailes
Australian Journal of Chemistry, 1959 , vol. 12, p. 173,186
反应条件
1: 1.) Et3N, glacial acetic acid, NaI, 2.) KI / 1.) dichloromethane, 0 deg C, 30 min; 2.) reflux, 1 h
2: 1.) NaBH4, glacial acetic acid, 2.) HCl, HCHO / 1.) ethanol, water, 0 deg C, 2 h; 2.) 80 deg C, 10 min
View Scheme
参考文献
Doleschall, Gabor; Seres, Peter
Acta Chimica Hungarica, 1987 , vol. 124, # 2 p. 209 - 216
