4-甲基-3-(4,4,5,5-四甲基-[1,3,2]二噁硼烷-2-基)苯甲酸合成路线 （共 3 条）
反应条件
potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in N,N-dimethyl-formamide T=100°C; 6 h; Inert atmosphere;
参考文献
Kyowa Hakko Kirin Co., Ltd.
Patent: EP2269993 A1, 2011 ;
Location in patent: Page/Page column 53 ;
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether; water
T=90°C; 4 h;
参考文献
J. URIACH Y COMPANIA S.A.
Patent: WO2007/339 A1, 2007 ;
Location in patent: Page/Page column 47 ;
WO 2007/000339 A1
反应条件
oxalyl dichloride; N,N-dimethyl-formamide in dichloromethane
T=20°C;
参考文献
GLAXO GROUP LIMITED
Patent: WO2007/147109 A2, 2007 ;
Location in patent: Page/Page column 206 ;
WO 2007/147109 A2
