1,5,6,7-四氢-1-甲基-4H-吲哚-4-酮合成路线 （共 6 条）
反应条件
in ethanol T=150°C; 12 h;
参考文献
Matsumoto, Masakatsu; Watanabe, Nobuko
Heterocycles, 1984 , vol. 22, # 10 p. 2313 - 2316
反应条件
toluene-4-sulfonic acid in toluene 12 h; Reflux;
参考文献
PHARMARESOURCES(SHANGHAI)CO., LTD.; CHEN, Ping; ZHOU, Ding; PRYDE, David; BELL, Andrew; LI, Tao; HE, Zhiliang; CAI, Zhen-Wei
Patent: WO2012/65062 A1, 2012 ;
Location in patent: Page/Page column 149 ;
反应条件
aluminium trichloride in chloroform T=60°C; 3 h;
参考文献
Harrowven; Dainty
Tetrahedron Letters, 1995 , vol. 36, # 37 p. 6739 - 6742
反应条件
1,4-diaza-bicyclo[2.2.2]octane in N,N-dimethyl-formamide T=90 - 92°C; 23 h;
参考文献
Laurila, Michael L.; Magnus, Nicholas A.; Staszak, Michael A.
Organic Process Research and Development, 2009 , vol. 13, # 6 p. 1199 - 1201
反应条件
1: conc. H2SO4 / ethyl acetate / 1 h 2: 92 percent / ethanol / 12 h / 150 °C View Scheme
参考文献
Matsumoto, Masakatsu; Watanabe, Nobuko
Heterocycles, 1984 , vol. 22, # 10 p. 2313 - 2316
反应条件
1: 2 N aq. NaHCO3 / Ambient temperature 2: conc. H2SO4 / ethyl acetate / 1 h 3: 92 percent / ethanol / 12 h / 150 °C View Scheme
参考文献
Matsumoto, Masakatsu; Watanabe, Nobuko
Heterocycles, 1984 , vol. 22, # 10 p. 2313 - 2316
