1-(4-甲氧苯基)-1H-吡咯合成路线 (共 21 条)
反应条件
in water T=150°C; Paal-Knorr condensation; 0.5 h; Microwave irradiation;
参考文献
Wilson, Matthew A.; Filzen, Gary; Welmaker, Gregory S.
Tetrahedron Letters, 2009 , vol. 50, # 34 p. 4807 - 4809
反应条件
copper (II) acetate monohydrate; caesium carbonate in N,N-dimethyl-formamide T=110°C; 24 h; Inert atmosphere;
参考文献
Xu, Zhong-Lin; Li, Hong-Xi; Ren, Zhi-Gang; Du, Wei-Yuan; Xu, Wei-Chang; Lang, Jian-Ping
Tetrahedron, 2011 , vol. 67, # 29 p. 5282 - 5288
反应条件
copper(l) iodide; 1-Hydroxymethyl-1H-benzotriazole; potassium tert-butylate in dimethyl sulfoxide T=110°C; Inert atmosphere;
参考文献
Verma, Akhilesh Kumar; Kesharwani, Tanay; Singh, Jaspal; Tandon, Vibha; Larock, Richard C.
Angewandte Chemie - International Edition, 2009 , vol. 48, # 6 p. 1138 - 1143
反应条件
copper(l) iodide; caesium carbonate in dimethyl sulfoxide T=110°C; 24 h;
参考文献
Reddy, V. Prakash; Kumar, A. Vijay; Rao, K. Rama
Tetrahedron Letters, 2011 , vol. 52, # 7 p. 777 - 780
反应条件
potassium fluoride; caesium carbonate; 2-(di-tert-butylphosphino)-2'-isopropylbiphenyl; palladium diacetate; carbon dioxide T=100°C; P=93086.6 Torr; 17 h;
参考文献
CAMBRIDGE UNIVERSITY TECHNICAL SERVICES LIMITED; ASTRAZENECA UK LIMITED
Patent: WO2005/90283 A1, 2005 ;
Location in patent: Page/Page column 29 ;
反应条件
copper(l) iodide; potassium carbonate in N,N-dimethyl-formamide T=20 - 110°C;
参考文献
Sreedhar; Arundhathi; Reddy, P. Linga; Kantam, M. Lakshmi
Journal of Organic Chemistry, 2009 , vol. 74, # 20 p. 7951 - 7954
反应条件
RuCl2(tricyclohexylphosphine)2(benzylidene); FeCl3·6H2O; oxygen in dichloromethane T=40°C; 24 h;
参考文献
Chen, Weiqiang; Wang, Jianhui
Organometallics, 2013 , vol. 32, # 6 p. 1958 - 1963
反应条件
MgI2 etherate in acetonitrile T=80°C; Clauson-Kaas pyrrole synthesis; chemoselective reaction;
参考文献
Zhang, Xingxian; Shi, Junchen
Tetrahedron, 2011 , vol. 67, # 5 p. 898 - 903
反应条件
potassium fluoride; caesium carbonate; 2-(di-tert-butylphosphino)-2'-isopropylbiphenyl; palladium diacetate; carbon dioxide T=75°C; P=93086.6 Torr; 17 h;
参考文献
Smith, Catherine J.; Tsang, Melanie W.S.; Holmes, Andrew B.; Danheiser, Rick L.; Tester, Jefferson W.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 20 p. 3767 - 3781
反应条件
sodium tetrahydroborate; sulfuric acid; water in tetrahydrofuran; methanol T=10 - 20°C; 1.5 h; Yield given;
参考文献
Verardo, Giancarlo; Dolce, Anna; Toniutti, Nicoletta
Synthesis, 1999 , # 1 p. 74 - 79