5-(2-甲氧基苯基)-1H-四唑合成路线 (共 5 条)
反应条件
Bu3SnN3 in xylene Cycloaddition; Heating;
参考文献
Norman, Derek P. G.; Bunnell, Aaron E.; Stabler, S. Russell; Flippin, Lee A.
Journal of Organic Chemistry, 1999 , vol. 64, # 25 p. 9301 - 9306
反应条件
1-lithio-2-methylnaphthalene in diethyl ether T=23°C; dealkylation; 48 h;
参考文献
Norman, Derek P. G.; Bunnell, Aaron E.; Stabler, S. Russell; Flippin, Lee A.
Journal of Organic Chemistry, 1999 , vol. 64, # 25 p. 9301 - 9306
反应条件
1,4-diaza-bicyclo[2.2.2]octane; sodium azide; palladium diacetate; sodium carbonate; zinc dibromide in N,N-dimethyl-formamide T=140°C; 32 h; Inert atmosphere;
参考文献
Zhu, Yizhong; Ren, Yiming; Cai, Chun
Helvetica Chimica Acta, 2009 , vol. 92, # 1 p. 171 - 175
反应条件
1: POCl3; Na2S2O5 2: NaN3; acetic acid; butan-1-ol View Scheme
参考文献
Herbst; Wilson
Journal of Organic Chemistry, 1957 , vol. 22, p. 1142,1145
反应条件
1: aqueous NH3 2: POCl3; Na2S2O5 3: NaN3; acetic acid; butan-1-ol View Scheme
参考文献
Herbst; Wilson
Journal of Organic Chemistry, 1957 , vol. 22, p. 1142,1145