反应条件
1: 93 percent / SOCl2 / 1.) 0 deg C to r.t., 2.) r.t., 16 h 2: 90 percent / DIBAL-H / tetrahydrofuran; toluene / 1.) -78 deg C, 1 h, 2.) -78 deg C to 0 deg C; 0 deg C, 1 h View Scheme
参考文献
Sumi, Kengo; Inoue, Yoshihiro; Nishio, Masahiro; Naito, Yasuhito; Hosoya, Takamitsu; Suzuki, Masaaki; Hidaka, Hiroyoshi
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 3 p. 831 - 834
