2-(4-异丁基苯基)丙醛合成路线 （共 31 条）
反应条件
sulfuric acid
0.25 h; Ambient temperature;
参考文献
Sugai, Saburo; Kodama, Takashi; Akaboshi, Sanya; Ikegami, Shiro
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 1 p. 99 - 105
反应条件
palladium in ethanol
参考文献
Sterling Drug Inc.
Patent: US3965105 A1, 1976 ;
反应条件
Dess-Martin periodane in dichloromethane
Inert atmosphere;
参考文献
Friest, Jacob A.; Maezato, Yukari; Broussy, Sylvain; Blum, Paul; Berkowitz, David B.
Journal of the American Chemical Society, 2010 , vol. 132, # 17 p. 5930 - 5931
反应条件
diisobutylaluminium hydride in diethyl ether; hexane
T=-78°C;
参考文献
Giacomini, Daria; Galletti, Paola; Quintavalla, Arianna; Gucciardo, Gabriele; Paradisi, Francesca
Chemical Communications, 2007 , # 39 p. 4038 - 4040
反应条件
1: 94 percent / LiAlH4 / diethyl ether / 4 h / 10 °C
2: 54 percent / dimethylsulfoxide, oxalyl chloride / CH2Cl2 / 1 h / -78 °C
View Scheme
参考文献
Neibecker, Denis; Reau, Regis; Lecolier, Serge
Journal of Organic Chemistry, 1989 , vol. 54, # 22 p. 5208 - 5210
参考文献
Hamari Chemicals, Ltd.
Patent: US4670607 A1, 1987 ;
反应条件
carbon tetrabromide; triphenylphosphine in dichloromethane
T=20°C; 8 h;
参考文献
Gong, Wanchun; Liu, Yun; Xue, Jijun; Xie, Zhixiang; Li, Ying
Chemistry Letters, 2012 , vol. 41, # 12 p. 1597 - 1599
反应条件
1: With LDBBA in tetrahydrofuran
T=0°C; Inert atmosphere;
2: With water; sodium hydroxide in tetrahydrofuran
0.5 h;
参考文献
Friest, Jacob A.; Maezato, Yukari; Broussy, Sylvain; Blum, Paul; Berkowitz, David B.
Journal of the American Chemical Society, 2010 , vol. 132, # 17 p. 5930 - 5931
反应条件
tetracarbonylbis(μ-chloro)dirhodium(I); hydrogen; 1,2,5-triphenyl-1H-phosphole; triethylamine in toluene
T=25°C; P=15001.2 Torr; 6 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Neibecker, Denis; Reau, Regis; Lecolier, Serge
Journal of Organic Chemistry, 1989 , vol. 54, # 22 p. 5208 - 5210
反应条件
sodium hydroxide; sodium sulfate in dichloromethane
参考文献
Hamari Chemicals, Ltd.
Patent: US4670607 A1, 1987 ;
