N*2*,N*2*-二乙基-1,2-丙二胺合成路线 (共 6 条)
反应条件
chloroformic acid ethyl ester; triethylamine
1.) DMF, 0 deg C, 30 min, 2.) room temp.; Yield given. Multistep reaction;
参考文献
Dostert; Imbert; Ancher; et al.
European Journal of Medicinal Chemistry, 1982 , vol. 17, # 5 p. 437 - 444
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Casy,A.F.; Wright,J.
Journal of the Chemical Society [Section] C: Organic, 1966 , p. 1167 - 1171
反应条件
1: LiAlH4 / diethyl ether
2: H2 / Pd-C / ethanol
View Scheme
参考文献
Casy,A.F.; Wright,J.
Journal of the Chemical Society [Section] C: Organic, 1966 , p. 1167 - 1171
反应条件
methanol; ammonia
T=100 - 120°C;
参考文献
Prelog; Rajner; Stern
Helvetica Chimica Acta, 1943 , vol. 26, p. 1176
反应条件
sodium hydroxide
T=70°C;
参考文献
Carbide and Carbon Chem. Corp.
Patent: US2364178 , 1943 ;
参考文献
Ciba
Patent: CH139446 , 1927 ;