4-乙酰氨基-2-甲基硝基苯合成路线 （共 22 条）
反应条件
Bi(NO3)3·5H2O in dichloromethane
T=23°C; regioselective reaction;
参考文献
Lu, Yang; Li, Yaming; Zhang, Rong; Jin, Kun; Duan, Chunying
Tetrahedron, 2013 , vol. 69, # 45 p. 9422 - 9427
反应条件
nitric acid; phosphorus pentoxide; silica gel
T=20°C; 0.0666667 h;
参考文献
Hajipour, Abdol Reza; Ruoho, Arnold E.
Tetrahedron Letters, 2005 , vol. 46, # 48 p. 8307 - 8310
反应条件
nitrogen(IV) oxide; ozone in chloroform
2 h; < 0 deg C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Suzuki, Hitomi; Ishibashi, Taro; Murashima, Takashi; Tsukamoto, Kenkichi
Tetrahedron Letters, 1991 , vol. 32, # 45 p. 6591 - 6594
反应条件
copper(I) nitrate trihydrate
参考文献
Coffey
Journal of the Chemical Society, 1926 , p. 3221
反应条件
2: NO2, O3, O2 / CHCl3 / 2 h / 0 °C
View Scheme
参考文献
Suzuki, Hitomi; Tatsumi, Atsuo; Ishibashi, Taro; Mori, Tadashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 4 p. 339 - 344
参考文献
Hodgson; Heyworth
Journal of the Chemical Society, 1949 , p. 1624
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McGookin; Swift
Journal of the Society of Chemical Industry, London, 1939 , vol. 58, p. 152
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de Vries
Recueil des Travaux Chimiques des Pays-Bas, 1942 , vol. 61, p. 647,658
反应条件
sulfuric acid; nitric acid; acetic acid
T=0°C; Nebenprod.: 2-Nitro-3-amino-toluol;
参考文献
Noelting; Stoecklin
Chemische Berichte, 1891 , vol. 24, p. 564
反应条件
1: aqueous alcohol; ammonia / 150 °C
2: sulfuric acid
View Scheme
参考文献
Kenner; Parkin
Journal of the Chemical Society, 1920 , vol. 117, p. 856
反应条件
1: fuming nitric acid
2: aqueous alcohol; ammonia / 150 °C
3: sulfuric acid
View Scheme
参考文献
Kenner; Parkin
Journal of the Chemical Society, 1920 , vol. 117, p. 856
参考文献
Kenner; Parkin
Journal of the Chemical Society, 1920 , vol. 117, p. 856
