tetrachloromethane; hexacarbonyl molybdenum T=120°C; 8 h;

1: sodium; isoamyl alcohol 2: petroleum ether; HCl View Scheme

1: sodium; isoamyl alcohol 2: petroleum ether; HCl View Scheme

sodium iodide in N,N-dimethyl-formamide T=65°C; 42 h;

1: 74 percent / NaI / dimethylformamide / 42 h / 65 °C 3: powdered sodium hydroxide / dioxane / 14 h / Ambient temperature; further solvents were also used 4: Adogen, sodium dithionite, NaHCO3 / cyclohexane; H2O / 2 h / Heating View Scheme

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1: 74 percent / NaI / dimethylformamide / 42 h / 65 °C 3: powdered sodium hydroxide / dioxane / 14 h / Ambient temperature; further solvents were also used 4: Adogen, sodium dithionite, NaHCO3 / cyclohexane; H2O / 2 h / Heating 5: pyridine / 4 h / Ambient temperature View Scheme

potassium fluoride; diethylene glycol T=120°C;