2-甲基-2-丙烯-1-醇合成路线 (共 240 条)
反应条件
sodium tetrahydroborate; carbon in tetrahydrofuran; water T=20°C; 0.0166667 h;
参考文献
Setamdideh, Davood; Zeynizadeh, Behzad
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2006 , vol. 61, # 10 p. 1275 - 1281
反应条件
lithium aluminium tetrahydride in diethyl ether T=-30°C; Reduction; 4 h;
参考文献
Werkhoven, Thekla M.; Siebum, Arjan H. G.; Lugtenburg, Johan
European Journal of Organic Chemistry, 2000 , # 11 p. 2113 - 2117
反应条件
zirconium tetra-n-propoxide in propan-1-ol T=-80 - 170°C; P=7.50075 - 15.0015 Torr; Product distribution / selectivity;
参考文献
US2010/197973 A1, ;
Page/Page column 2; 3 ;
反应条件
in methanol; potassium hydroxide
反应条件
(1R,2S)-(+)-1-cyclohexyl-2-phenyl-2-(N-morpholino)ethanol in hexane; toluene T=20°C; 3 h; Title compound not separated from byproducts.;
参考文献
Organic Letters, , vol. 4, # 13 p. 2133 - 2136
反应条件
trilithium phosphate T=210°C; 3 h; 110 - 180 degC , ΔG, ΔH, E(activ.); KineticsThermodynamic data;
参考文献
Journal of applied chemistry of the USSR, , vol. 57, # 9 pt 2 p. 1915 - 1919
反应条件
dihydrogen peroxide in pyridine; dichloromethane T=0°C; 0.333333 h; Yield given;
参考文献
Tetrahedron Letters, , vol. 22, # 52 p. 5285 - 5288
反应条件
1: in tetrahydrofuran; diethyl ether T=-20 - 20°C; Inert atmosphere; 2: With sulfuric acid; water in tetrahydrofuran; diethyl ether T=20°C; Inert atmosphereMolecular sieve;
参考文献
Chemistry - A European Journal, , vol. 17, # 47 p. 13341 - 13348
反应条件
aluminum oxide; copper(II) sulfate T=225°C; P=760 Torr;
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Journal of the American Chemical Society, , vol. 78, p. 4377