反应条件
1: 3-ethyl-1-butyl bromide With magnesium
2: acrylic acid methyl ester With 4-(N,N-dimethlyamino)pyridine; chloro-trimethyl-silane; copper(I) bromide dimethylsulfide complex in tetrahydrofuran
T=-78°C; 3.5 h;
参考文献
Dickschat, Jeroen S.; Bruns, Hilke; Riclea, Ramona
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, p. 1697 - 1712
