3-氨基-2-甲氧基-苯甲酸甲酯合成路线 （共 3 条）
反应条件
palladium 10 on activated carbon; hydrogen in tetrahydrofuran
T=40°C; 3 h;
参考文献
Qin, Bo; Chen, Xiuying; Fang, Xiao; Shu, Yingying; Yip, Yeow Kwan; Yan, Yan; Pan, Siyan; Ong, Wei Qiang; Ren, Changliang; Su, Haibin; Zeng, Huaqiang
Organic Letters, 2008 , vol. 10, # 22 p. 5127 - 5130
反应条件
hydrogen; palladium 10 on activated carbon in 1,4-dioxane; ethanol; water
5.5 h;
参考文献
SHIONOGI and CO., LTD.
Patent: EP1375486 A1, 2004 ;
Location in patent: Page 143; 144 ;
反应条件
1: With pyridine; trifluorormethanesulfonic acid; tetra-n-butylammonium tetrafluoroborate in acetonitrile
T=25°C; Electrochemical reaction;
2: With piperidine in acetonitrile
T=80°C; 12 h; Electrochemical reaction; Overall yield = 92 percent;
参考文献
Morofuji, Tatsuya; Shimizu, Akihiro; Yoshida, Jun-Ichi
Journal of the American Chemical Society, 2013 , vol. 135, # 13 p. 5000 - 5003
