3-苯基-3,4-二氢-2H-苯并[e][1,3]恶嗪合成路线 （共 5 条）
反应条件
in toluene
4 h; Heating / reflux;
参考文献
HENKEL CORPORATION
Patent: WO2008/156443 A1, 2008 ;
Location in patent: Page/Page column 20 ;
反应条件
in ethanol
5 h; Heating;
参考文献
Andreu; Ronda
Synthetic Communications, 2008 , vol. 38, # 14 p. 2316 - 2329
反应条件
1: 95 percent / NaBH4 / methanol / 0.5 h / Ambient temperature
2: 94 percent / ethanol / 5 h / Heating
View Scheme
参考文献
Joglekar, S. J.; Samant, S. D.
Journal of the Indian Chemical Society, 1988 , vol. 65, p. 110 - 111
反应条件
1: methanol / 0.5 h / 20 - 25 °C
2: sodium tetrahydroborate / methanol / 0 - 30 °C
3: methanol; water / 65 - 68 °C
View Scheme
参考文献
Shukla, Davender Kumar; Rani, Manju; Khan, Arif Ali; Tiwari, Kavita; Gupta, Rajinder K.
Asian Journal of Chemistry, 2013 , vol. 25, # 11 p. 5921 - 5924
反应条件
1: methanol / 0.5 h / 20 - 25 °C
2: sodium tetrahydroborate / methanol / 0 - 30 °C
3: methanol; water / 65 - 68 °C
View Scheme
参考文献
Shukla, Davender Kumar; Rani, Manju; Khan, Arif Ali; Tiwari, Kavita; Gupta, Rajinder K.
Asian Journal of Chemistry, 2013 , vol. 25, # 11 p. 5921 - 5924
