anhydrous sodium hydrogen carbonate; sodium hydrogen sulphite; 3-chloro-benzenecarboperoxoic acid in dichloromethane; water

potassium iodide; sodium carbonate

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potassium carbonate in acetonitrile 3 h; Reflux;

1: 80.8 percent / NaBH4 / ethanol / 30 - 35 °C 2: 84 percent / SOCl2, triethylbenzylammonium chloride / 1 h / 60 °C 3: 472 g / K2CO3 / acetonitrile / 12 h / Heating 4: 83.2 percent / LiAlH4 / diethyl ether / 1 h / Heating View Scheme