1-(4-(溴甲基)苯基)乙酮合成路线 （共 16 条）
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in acetonitrile T=90°C; Wohl-Ziegler bromination; 1.5 h;
参考文献
Pieck, J. Carsten; Kuch, David; Grolle, Friederike; Linne, Uwe; Haas, Clemens; Carell, Thomas
Journal of the American Chemical Society, 2006 , vol. 128, # 5 p. 1404 - 1405
反应条件
N-bromosuccinmide in water T=25°C; Wohl-Ziegler bromination; 25 h;
参考文献
Podgorsek, Ajda; Stavber, Stojan; Zupan, Marko; Iskra, Jernej
Tetrahedron, 2009 , vol. 65, # 22 p. 4429 - 4439
反应条件
N-bromosuccinmide; triphenylphosphine in tetrahydrofuran T=0°C; 1 h; Inert atmosphere;
参考文献
Wang, Zhengqiang; Tang, Jing; Salomon, Christine E.; Dreis, Christine D.; Vince, Robert
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 12 p. 4202 - 4211
反应条件
in toluene 12 h; Heating;
参考文献
Rodi, Youssef Kandri; Lopez, Lucien; Bellan, Jacques; Barrans, Jean; Essassi, El Moktar
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 85, # 1-4 p. 225 - 231
反应条件
1: sodium azide; acetic acid / ethanol; water / 74 h / 4 °C 2: toluene / 15 h / Photolysis View Scheme
参考文献
Ranaweera, Ranaweera A. A. Upul; Zhao, Yu; Muthukrishnan, Sivaramakrishnan; Keller, Christopher; Gudmundsdottir, Anna D.
Australian Journal of Chemistry, 2010 , vol. 63, # 12 p. 1645 - 1655
反应条件
1: sodium azide; acetic acid / ethanol; water / 74 h / 4 °C 2: chloroform / Photolysis View Scheme
参考文献
Ranaweera, Ranaweera A. A. Upul; Zhao, Yu; Muthukrishnan, Sivaramakrishnan; Keller, Christopher; Gudmundsdottir, Anna D.
Australian Journal of Chemistry, 2010 , vol. 63, # 12 p. 1645 - 1655
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl acetamide T=90°C; 1 h; Reagent/catalystSolventTemperature; chemoselective reaction;
参考文献
Rao, Maddali L. N.; Dhanorkar, Ritesh J.
RSC Advances, 2013 , vol. 3, # 19 p. 6794 - 6798
反应条件
1: 67 percent / dioxane; H2O / 2 h / 90 °C 2: 47 percent / aq. acetic acid; sulfuric acid / 1.5 h / 100 °C View Scheme
参考文献
Xu; Wan
Chemical Communications, 2000 , # 21 p. 2147 - 2148
反应条件
1: sodium azide; acetic acid / ethanol; water / 74 h / 4 °C 2: chloroform / 0.18 h / Photolysis View Scheme
参考文献
Ranaweera, Ranaweera A. A. Upul; Zhao, Yu; Muthukrishnan, Sivaramakrishnan; Keller, Christopher; Gudmundsdottir, Anna D.
Australian Journal of Chemistry, 2010 , vol. 63, # 12 p. 1645 - 1655
反应条件
water; calcium carbonate in 1,4-dioxane 15 h; Heating;
参考文献
Journal of the American Chemical Society, , vol. 121, # 10 p. 2085 - 2096
