3-(2-甲基-1,3-二氧烷-2-基)苯胺合成路线 （共 7 条）
反应条件
hydrogen; palladium on activated charcoal in ethanol T=20°C; Catalytic hydrogenation; P=37503 Torr; 0.5 h;
参考文献
Petersen, Lars; Jensen, Knud J.; Nielsen, John
Synthesis, 1999 , # 10 p. 1763 - 1766
反应条件
pyrrolidine; samarium diiodide; water in tetrahydrofuran T=20°C; Inert atmosphere; chemoselective reaction;
参考文献
Ankner, Tobias; Hilmersson, Goeran
Organic Letters, 2009 , vol. 11, # 3 p. 503 - 506
反应条件
sodium hydroxide in ethanol Heating;
参考文献
Zhang; Haemers; Vanden Berghe; Pattyn; Bollaert; Levshin
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 3 p. 673 - 683
反应条件
in diethyl ether; ethylene glycol; Petroleum ether; benzene
参考文献
Institut National de la Sante et de la Recherche Medical; Societe Civile Bioprojet
Patent: US6248765 B1, 2001 ;
反应条件
1: 89 percent / p-TsOH / benzene / 16 h / Heating 2: 93 percent / H2 / 5 percent Pd/C / ethanol / 0.5 h / 20 °C / 37503 Torr View Scheme
参考文献
Petersen, Lars; Jensen, Knud J.; Nielsen, John
Synthesis, 1999 , # 10 p. 1763 - 1766
反应条件
1: p-CH3C6H4SO3H*H2O / toluene / Heating 2: 72 percent / 10percent aq. NaOH / ethanol / Heating View Scheme
参考文献
Zhang; Haemers; Vanden Berghe; Pattyn; Bollaert; Levshin
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 3 p. 673 - 683
反应条件
1: CF3CO2H / Heating 2: p-CH3C6H4SO3H*H2O / toluene / Heating 3: 72 percent / 10percent aq. NaOH / ethanol / Heating View Scheme
参考文献
Zhang; Haemers; Vanden Berghe; Pattyn; Bollaert; Levshin
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 3 p. 673 - 683
