2-溴-2',3',4',5',6'-五氟苯乙酮合成路线 (共 9 条)
反应条件
copper(ll) bromide in chloroform; ethyl acetate 4 h; Heating; Title compound not separated from byproducts;
参考文献
Henry, Ronald A.; Hollins, Richard A.; Lowe-Ma, Charlotte; Moore, Donald W.; Nissan, Robin A.
Journal of Organic Chemistry, 1990 , vol. 55, # 6 p. 1796 - 1801
反应条件
1: diethyl ether / Heating 2: CrO3, AcOH View Scheme
参考文献
Coe,P.L. et al.
Journal of the Chemical Society [Section] C: Organic, 1966 , p. 597 - 603
反应条件
chromium(VI) oxide; acetic acid
参考文献
Coe,P.L. et al.
Journal of the Chemical Society [Section] C: Organic, 1966 , p. 597 - 603
参考文献
Chapman,N.B. et al.
Journal of the Chemical Society [Section] C: Organic, 1967 , p. 293 - 296
参考文献
Chapman,N.B. et al.
Journal of the Chemical Society [Section] C: Organic, 1967 , p. 293 - 296
反应条件
1: P2O5 / 200 °C 3: Br2 View Scheme
参考文献
Chapman,N.B. et al.
Journal of the Chemical Society [Section] C: Organic, 1967 , p. 293 - 296
反应条件
T=140 - 150°C; 1.66667 h; Title compound not separated from byproducts;
参考文献
Maslennikov, I. G.; Matus, L. I.; Kirichenko, L. N.; Lavrent'ev, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 2 p. 513,467
反应条件
T=140 - 150°C; 1.66667 h; Title compound not separated from byproducts;
参考文献
Maslennikov, I. G.; Matus, L. I.; Kirichenko, L. N.; Lavrent'ev, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 2 p. 513,467
反应条件
phosphonic acid dimethyl ester in acetonitrile E(a), var. temperatures; KineticsThermodynamic dataRate constant;
参考文献
Maslennikov, I. G.; Matus, L. I.; Lavrent'ev, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 5.2 p. 1089 - 1091,890 - 891