4-氨基-N,N-二乙基苯甲酰胺合成路线 (共 5 条)
反应条件
hydrazine hydrate; nickel in ethanol 4 h; Heating;
参考文献
Srivastava, Neera; Gupta, Anurag Ateet; Gupta, Anil K. Sen
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, p. 787 - 789
反应条件
tris(dibenzylideneacetone)dipalladium (0); lithium hexamethyldisilazane; 2-dicyclohexylphosphino-1,1'-biphenyl in 1,4-dioxane T=80°C; 15 h;
参考文献
Huang; Buchwald
Organic letters, 2001 , vol. 3, # 21 p. 3417 - 3419
反应条件
MoO2[S2CNEt2]2; phenyl silane in toluene T=100°C; 5 h;
参考文献
Maddani, Mahagundappa R.; Moorthy, Saravana K.; Prabhu, Kandikere R.
Tetrahedron, 2010 , vol. 66, # 1 p. 329 - 333
反应条件
1: 50 - 60 °C 2: tin (II)-chloride; aqueous hydrochloric acid; acetic acid View Scheme
参考文献
PROLYNX LLC; ASHLEY, Gary, W.; SANTI, Daniel, V.
Patent: WO2013/36857 A1, 2013 ;
反应条件
in ethanol; water Heating;
参考文献
Husain, M. I.; Shukla, Sarveshwar
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 761 - 764