1-氯-4-(乙基硫代)苯合成路线 (共 23 条)
反应条件
isopentyl nitrite in 1,4-dioxane; 1,2-dichloro-ethane 0.75 h; Heating;
参考文献
Nakayama, Juzo; Fujita, Toko; Hoshino, Masamatsu
Chemistry Letters, 1983 , p. 249 - 250
反应条件
potassium hydroxide in ethanol
3 h; Ambient temperature;
参考文献
Aitken, R. Alan; Armstrong, Jill M.; Drysdale, Martin J.; Ross, Fiona C.; Ryan, Bruce M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1999 , # 5 p. 593 - 604
反应条件
sodium hydroxide
6 h; Heating;
参考文献
Inbar, Shai; Linschitz, Henry; Cohen, Saul G.
Journal of the American Chemical Society, 1982 , vol. 104, # 6 p. 1679 - 1682
反应条件
water; hydroxymethanesulfinic acid sodium salt; potassium carbonate in N,N-dimethyl-formamide
0.25 h;
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Synthesis, 2007 , # 1 p. 85 - 91
反应条件
potassium phosphate; copper(l) iodide; tetrabutylammomium bromide in N,N-dimethyl-formamide
Ullmann coupling; 22 h; Heating;
参考文献
Buranaprasertsuk, Pongchart; Chang, Joyce Wei Wei; Chavasiri, Warinthorn; Chan, Philip Wai Hong
Tetrahedron Letters, 2008 , vol. 49, # 12 p. 2023 - 2025
反应条件
water; hydroxymethanesulfinic acid sodium salt; potassium carbonate in N,N-dimethyl-formamide
0.5 h;
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Synthesis, 2007 , # 1 p. 85 - 91
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=120°C; 1 h;
参考文献
Chianelli, Donatella; Testaferri, Lorenzo; Tiecco, Marcello; Tingoli, Marco
Synthesis, 1982 , # 6 p. 475 - 478
反应条件
T=500 - 600°C; P=0.01 Torr; 2.77778E-06 h;
参考文献
Aitken, R. Alan; Drysdale, Martin J.; Ryan, Bruce M.
Journal of the Chemical Society, Chemical Communications, 1994 , # 7 p. 805 - 806
反应条件
T=600°C; P=0.01 Torr; 2.77778E-06 h;
参考文献
Aitken, R. Alan; Drysdale, Martin J.; Ryan, Bruce M.
Journal of the Chemical Society, Chemical Communications, 1994 , # 7 p. 805 - 806
反应条件
aluminum oxide; sodium hypophosphite; iron(II) sulfate
0.0666667 h; microwave irradiation;
参考文献
Meshram; Ganesh; Babu, K. Ramesh; Eeshwaraiah; Yadav
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 1 p. 193 - 195