H2O in diethyl ether byproducts: HCl; partial hydrolysis of (C6H5)2SiCl2 in ether with H2O/dioxane; sepn. of HCl by a dry stream of N2;; extraction with n-heptane;;
参考文献
Burkhard
Journal of the American Chemical Society, 1945 , vol. 67, p. 2173 Anm.6
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Gmelin Handbook: Si: MVol.C, 106, page 292 - 295
pyridine; sodium hydrogencarbonate in toluene T=20°C; 3 h;
参考文献
Kipping
Journal of the Chemical Society, 1912 , vol. 101, p. 2108
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Kipping; Murray
Journal of the Chemical Society, 1928 , p. 1428,1430
