1,4,4a,8a-四氢-内-1,4-亚甲基萘-5,8-二酮合成路线 （共 7 条）
反应条件
1: 82 percent / NaBH4, CeCl3 2: 1.) n-BuLi 3: 26 percent / (dba)3Pd*CHCl3, triisopropyl phosphite / 6 h / Ambient temperature View Scheme
参考文献
Trost, Barry M.; Tometzki, Gerald B.
Journal of Organic Chemistry, 1988 , vol. 53, # 4 p. 915 - 917
反应条件
T=54.6 - 78.6°C; Kinetics;
参考文献
Journal of the Chemical Society, , p. 375,376, 377
反应条件
T(p-OCH3)PPFeCl; dihydrogen peroxide; 1-n-butyl-3-methylimidazolium hexafluorophosphate in dichloromethane; acetonitrile T=20°C; 3 h; chemoselective reaction;
参考文献
Singh, Pradeep Pratap; Ambika; Chauhan
New Journal of Chemistry, 2012 , vol. 36, # 3 p. 650 - 655
反应条件
pyridine T=20°C; 168 h;
参考文献
Stoermer, Martin J.; Butler, Douglas N.; Warrener, Ronald N.; Weerasuria; Fairlie, David P.
Chemistry - A European Journal, 2003 , vol. 9, # 9 p. 2068 - 2071
反应条件
ethanol; palladium
Hydrogenation;
参考文献
Diels; Blom; Koll
Justus Liebigs Annalen der Chemie, 1925 , vol. 443, p. 247
反应条件
samarium diiodide; oxygen in tetrahydrofuran
Ambient temperature1.) 1 h; 2.) 15 min;
参考文献
Pandey; Saravanan; Rao; Nagamani; Kumar
Tetrahedron Letters, 1995 , vol. 36, # 7 p. 1145 - 1148
反应条件
samarium diiodide in tetrahydrofuran
1 h; Ambient temperature;
参考文献
Pandey; Saravanan; Rao; Nagamani; Kumar
Tetrahedron Letters, 1995 , vol. 36, # 7 p. 1145 - 1148
