1,5-二碘-3-甲基戊烷合成路线 （共 4 条）
反应条件
phosphorus; iodine
T=45°C; 42 h; Cooling with ice bath;
参考文献
Jahangir, Alam; Lynch, Stephen M.; Soth, Michael; Yang, Hanbiao
Patent: US2011/71179 A1, 2011 ;
Location in patent: Page/Page column 31 ;
反应条件
sodium iodide in acetone
Substitution; 3 h; Heating;
参考文献
Avis; Boulanger; Belanger
Journal of Chemical Ecology, 2000 , vol. 26, # 4 p. 987 - 1000
反应条件
1: 44 percent / LiAlH4 / tetrahydrofuran / 2 h / 20 °C
2: 73 percent / PBr3 / 20 h / -10 - 20 °C
3: 89 percent / NaI / acetone / 3 h / Heating
View Scheme
参考文献
Avis; Boulanger; Belanger
Journal of Chemical Ecology, 2000 , vol. 26, # 4 p. 987 - 1000
反应条件
(i) NaNH2, (ii) /BRN= 1839597/, MeCN; Multistep reaction;
参考文献
Cope,A.C.; Gale,D.M.
Journal of the American Chemical Society, 1963 , vol. 85, p. 3743 - 3747
