5-甲基-4-异噁唑甲酸乙酯合成路线 (共 6 条)
反应条件
sulfuric acid in o-tolyl acetic acid
参考文献
Ray, Anup Kumar; Patel, Hiren Kumar V.; Patel, Mahendra R.
Patent: US2003/139606 A1, 2003 ;
反应条件
1: 15 percent / NaOH / aq. ethanol / Ambient temperature 2: 82 percent / aq. HCl / 0.5 h / Heating View Scheme
参考文献
Alberola; Antolin; Gonzalez; et al.
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 4 p. 1035 - 1038
反应条件
sodium ethanolate in diethyl ether; ethanol 12 h; Ambient temperature;
参考文献
Schenone, Pietro; Fossa, Paola; Menozzi, Giulia
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 2 p. 453 - 457
参考文献
Yasuda
Yakugaku Zasshi, 1959 , vol. 79, p. 836
Chem.Abstr., 1960 , p. 1493
反应条件
1: 270 g / conc. HCl / acetic acid; H2O / 10 h / Heating 2: 47 percent / thionyl chloride / 3 h / Heating View Scheme
参考文献
Ye, Dong-Ju
Asian Journal of Chemistry, 2010 , vol. 22, # 2 p. 1503 - 1506
反应条件
1: NaOH 2: 20 percent / hydroxylamine hydrochloride / H2O / 3 h / Heating View Scheme
参考文献
Alberola; Antolin; Gonzalez; et al.
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 4 p. 1035 - 1038