5-硝基-Alpha-四氢萘酮合成路线 （共 15 条）
反应条件
trifluorormethanesulfonic acid T=130°C; 0.75 h;
参考文献
BAYER AG
Patent: EP1369412 A1, 2003 ;
Location in patent: Page 6 ;
反应条件
1: With AlCl3, aluminium chloride in CS2 (carbon disulfide) T=15 - 20°C; 4 h; 2: With water in CS2 (carbon disulfide); dichloromethane
参考文献
BAYER AG
Patent: EP1369412 A1, 2003 ;
Location in patent: Page 6, 7 ;
反应条件
sulfuric acid; nitric acid T=0°C; 1 h;
参考文献
Riedel,J. D.
Patent: DE408665 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 466
反应条件
chromium(VI) oxide; acetic acid
参考文献
Nakamura
Yakugaku Zasshi, 1941 , vol. 61, p. 292,294; dtsch. Ref. S. 108
Chem.Abstr., 1950 , p. 9389
反应条件
ammonium nitrate; trifluoroacetic anhydride in acetonitrile T=20°C; 5 h;
参考文献
Zheng; Jing; Patil; Lei; Feller; Miller
Medicinal Chemistry Research, 2001 , vol. 10, # 5 p. 318 - 327
参考文献
Schelhaas, Michael; Joschek, Katrin; Jautelat, Manfred; Zechlin, Joachim; Wastian, Dietmar
Patent: US2002/103401 A1, 2002 ;
反应条件
in xylene 24 h; Heating;
参考文献
Takeuchi, Naoki; Ohki, Junji; Tobinaga, Seisho
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 2 p. 481 - 487
参考文献
Riedel,J. D.
Patent: DE397150 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 460
参考文献
Riedel,J. D.
Patent: DE408665 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 466
反应条件
palladium on activated carbon in diethylene glycol dimethyl ether T=130°C; 18 h;
参考文献
US2004/143137 A1, ;
Page 4 ;
