1,1-二(2,2-二硝基丙氧基)乙烷合成路线 （共 4 条）
反应条件
sodium hydroxide; potassium hexacyanoferrate(III); sodium nitrite in methanol; dichloromethane; water
T=5 - 25°C;
参考文献
Dimension Technology Chemical Systems, Inc.
Patent: US2009/216049 A1, 2009 ;
Location in patent: Page/Page column 7-8; 4 ;
反应条件
sodium hydroxide; potassium hexacyanoferrate(III); sodium nitrite in methanol; water
T=4 - 21°C; 2 h; Product distribution / selectivity;
参考文献
Dimension Technology Chemical Systems, Inc.
Patent: US2009/216049 A1, 2009 ;
Location in patent: Page/Page column 9 ;
反应条件
boron trifluoride diethyl etherate
参考文献
Coburn,M.D.
Synthesis, 1977 , p. 570
反应条件
sodium hydrogen sulphate
T=140 - 150°C; P=0.06 Torr;
参考文献
Coburn,M.D.
Synthesis, 1977 , p. 570
