反应条件
1: 99 percent / Na2CO3, NaI / dimethylformamide / 6 h / 20 - 65 °C 2: 83 percent / tetrahydrofuran / 12 h / Ambient temperature 3: methanesulfonyl azide, Et3N / acetonitrile 4: aq. LiOH / acetonitrile / 20 h / Ambient temperature View Scheme
参考文献
Padwa, Albert; Austin, David J.; Price, Alan T.; Semones, Mark A.; Doyle, Michael P.; Protopopova, Marina N.; Winchester, William R.; Tran, Andrea
Journal of the American Chemical Society, 1993 , vol. 115, # 19 p. 8669 - 8680